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K2CO3 Catalyzed using synthesis of mikanecic acid diesters from baylis hillman adducts formed using ticl4

Author:

andhikumar, R. and Dr. Subramani, K. N

Subject Area:

Physical Sciences and Engineering

Abstract:

A novel method for the synthesis of a terpenoid, Mikanecic acid diesters from Baylis-Hillman adducts, (alkyl-3-hydroxy-2-methylenepropanoates by treatment with aldehyde react with various acrylates catalyzed by TiCl4) which on treatment with potassium carbonate led directly to the formation of Mikanecic acid diesters, through Diels-Alder type self-dimerization of 1,3-butadiene-2-carboxylate is reported using with potassium carbonate. The product is obtained in good yield.

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