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Preparation of Thiourea based Imidazoline inhibitors

Author: 
Changshan Huang, Jinying Wu, Huiwu Xu, Min Zhang, Min Chen, MianXue, Xiaoguang Zhang, Guangxiu Cao and Can Huang
Subject Area: 
Physical Sciences and Engineering
Abstract: 

Imidazoline quaternary-ammonium-salt corrosion inhibitor and thioureido-imidazoline quaternary-ammonium-salt compound corrosion inhibitor were synthesized using oleic acid, diethylenetriamine, benzyl chloride and thiourea as theraw materials. The resulting samples were characterized by static weight-loss method, electrochemical polarization curve, X-ray photoelectron spectrometry (XPS) as well as scanning electron microscope (SEM). The electrochemical characteristics of the inhibitors’ inhibition towards carbon dioxide corrosion were investigated, the major constituents of the protective film formed on the surface of A3 carbon steel by thioureido-imidazoline compound corrosion inhibitor were analyzed, and the corrosion inhibiting mechanism for thioureido-imidazoline in hypersaline was explored. The results indicated that thioureido-imidazoline compound corrosion inhibitor had better corrosion inhibiting effect than imidazoline and can efficiently inhibit the corrosion of A3 carbon steel by CO2-saturated hypersaline water.

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