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Preparation, characterization and biological study of heterocyclic azo-schiff base compound and some of its metal complexes

Author: 
Zainab. J. Mohammed, Abbas. H. Al-Khafagy and Abid Allah. M. Ali
Subject Area: 
Physical Sciences and Engineering
Abstract: 

A new series of transition metal complexes of Co(II), Ni(II), Cu(II), Zn(II) and Cd(II), have been prepared from the azo-schiff base ligand (L) formed by coupling reaction of 1-(4-Aminophenyl)ethlidene-3-nitroaniline diazonium chloride with 4,5-diphenyl imidazole. The structural features have been arrived from their elemental analyses, magnetic susceptibility, molar conductivity, IR and UV-Vis spectral studies. The data show that the complexes have composition of [M(L)2Cl2] type M= Co(II), Ni(II), Cu(II), Zn(II) and Cd(II). The magnetic susceptibility and UV-Vis spectral data of the complexes suggest octahedral geometry around all the central metal ions. The invitro antibacterial activities of the synthesized compounds have been tested against the gram positive and gram negative bacteria,s. The activity data show that the metal complexes higher antibacterial activity than the free ligand.

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